TABLE 1.
Crystallographic information
Values in parentheses are for the highest resolution shell.
| ROP5BI-IRGa6-GDPa | ROP5CI-IRGa6-GDPb | |
|---|---|---|
| Data collection | ||
| Space group | P 1 | P 1 |
| Cell dimensions | ||
| a, b, c (Å) | 52.6, 54.7, 85.6 | 53.4, 53.7, 86.8 |
| α, β, γ (degrees) | 99.0, 106.6, 106.9 | 104.7, 95.3, 111.0 |
| Resolution (Å) | 1.70 Å | 1.72 Å |
| Rmerge | 5.8 (183.1) | 9.2 (202.8) |
| I/σI | 19.19 (1.15) | 19.43 (1.52) |
| CC(1/2) (52) | 100.0 (53.7) | 100.0 (65.9) |
| Completeness (%) | 99.5 (99.6) | 99.9 (99.9) |
| Redundancy | 8.07 (7.61) | 13.8 (13.7) |
| Refinement | ||
| Resolution (Å) | 1.70 | 1.72 |
| No. of reflections | 92,476 | 90,512 |
| Rwork/Rfree | 0.1923/0.2277 | 0.1951/0.2298 |
| No. of atoms | 6647 | 6676 |
| Protein | 6081 | 6065 |
| Ligand/ion | 83 | 96 |
| Water | 483 | 515 |
| B-factors | 38.00 | 35.90 |
| Protein | 37.50 | 35.50 |
| Ligand/ion | 31.52 | 38.32 |
| Water | 44.80 | 41.10 |
| RMSD | ||
| Bond lengths (Å) | 0.008 | 0.007 |
| Bond angles (degrees) | 1.106 | 1.128 |
a Three independent data sets were merged.
b Four independent data sets were merged.