Skip to main content
. Author manuscript; available in PMC: 2014 Nov 20.
Published in final edited form as: Bioconjug Chem. 2013 Nov 7;24(11):1784–1789. doi: 10.1021/bc400322h

Figure 4.

Figure 4

Synthesis and analysis of functionalized lipid building blocks. (A) Synthesis of DSPE-PEG2k; Reagents and conditions: (i) TCO-NHS, Et3N, DCM, room temperature, 5 h, Yield: 47%; (B) Synthesis of [18F]-FDP; Reagents and conditions: (ii) Acetonitrile, 120 °C, 20 min, dcRCY: 40% ± 5%, RCP: 96%; (C) ESI-MS analysis of DSPE-PEG2k-TCO versus DSPE-PEG2k; (D) iTLC of [18F]-FDP;