. Author manuscript; available in PMC: 2011 Mar 31.

Published in final edited form as: J Am Chem Soc. 2010 Mar 31;132(12):4295–4309. doi: 10.1021/ja910186u

Table 1.

Alignment tensors for the GB3 mutants in liquid crystalline Pf1.^a

	D_a (Hz)	R	α^b	β^b	γ^b
K19AV42ED47K	24.0	0.253	82.7	94.2	294
K19ED40NV42E	−12.4	0.222	89.9	336	133
K4AK19EV42E-C-histag	8.61	0.461	162	258	213
K4AK19EV42E-N-histag	18.5	0.179	123	256	184
T11KK19AV42E	20.0	0.300	102	246	220
K4AK19EV42E	10.3	0.551	162	251	23.0

The RDCs are fitted to the N-H orientations determined previously ⁶⁵ that were aligned relative to the molecular frame of PDB entry 2OED⁶¹ (SI, Table S8).

The angles reported are z-y-z convention Euler angles needed to rotate the molecular frame to the alignment tensor frame.⁷⁵