Fig. 5.
Two-dimensional NMR of Rnq1153–405. (A) Aliphatic region of 2D 13C–13C spectrum of U–15N,13C–Rnq1153–405 fibrils, with partial residue-type assignments of Cα/Cβ crosspeaks, obtained at a 17.00-kHz MAS frequency with a total of 55,296 scans and a maximum t1 value of 4.896 ms. Contour levels increase by successive factors of 1.5. (B) One-dimensional slices from the 2D spectrum, at positions indicated by dashed lines.
